{"id":118529,"date":"2022-06-22T12:27:47","date_gmt":"2022-06-22T16:27:47","guid":{"rendered":"http:\/\/www.bu.edu\/eng\/?page_id=118529"},"modified":"2024-09-17T13:23:41","modified_gmt":"2024-09-17T17:23:41","slug":"mse-core-research-facility","status":"publish","type":"page","link":"https:\/\/www.bu.edu\/eng\/academics\/departments-and-divisions\/materials-science-engineering\/research\/mse-core-research-facility\/","title":{"rendered":"MSE Core Research Facility"},"content":{"rendered":"<p>The Materials Science &amp; Engineering Core Research Facility was officially commissioned in June 2012. Since that time, it has grown to house multiple core pieces of equipment for the Materials Science &amp; Engineering and Photonics Center community.<\/p>\n<p>Address: 8 Saint Mary\u2019s St., Rooms 603 &amp; 605, Boston, MA 02215<br \/>\nLab Oversight: Professor David Bishop, djb1@bu.edu, Tel: (617) 358-4080<\/p>\n<h2>NEW Pulsed Laser Deposition (PLD) System from NMB Design arrived Fall 2024.<\/h2>\n<p>The newly purchased Pulsed Laser Deposition (PLD) System from NMB supports epitaxial oxide growth on crystal substrates, 6 targets, 1000 degrees celsius substrate heating, in-situ RHEED, and load lock.<\/p>\n<div class=\"bu-slideshow-container mse-research-facility autoplay\" id=\"bu-slideshow-container-139697\" data-slideshow-name=\"mse-research-facility\" data-slideshow-delay=\"3000\" style=\"width: auto; \"><div class='slideshow-loader active'><div class='loader-animation'><\/div><p>loading slideshow...<\/p><\/div><div class=\"bu-slideshow-slides\"><ul class=\"bu-slideshow transition-slide\" id=\"bu-slideshow-139697\"><li id=\"bu-slideshow-139697_0\" class=\"slide \"><div class=\"bu-slide-container slide-caption-bottom-right\"><img src=\"\/eng\/files\/2023\/05\/N8-Horizon-261x636-1.jpg\" alt=\"N8 Horizon System\" \/><div class=\"bu-slide-caption caption-bottom-right\"><p class=\"bu-slide-caption-title\">N8 Horizon System<\/p><\/div><\/div><\/li><li id=\"bu-slideshow-139697_1\" class=\"slide \"><div class=\"bu-slide-container slide-caption-bottom-right\"><img src=\"\/eng\/files\/2023\/05\/mic-636x477-1.png\" alt=\"D8 Discover System\" \/><div class=\"bu-slide-caption caption-bottom-right\"><p class=\"bu-slide-caption-title\">D8 Discover System<\/p><\/div><\/div><\/li><li id=\"bu-slideshow-139697_2\" class=\"slide \"><div class=\"bu-slide-container slide-caption-bottom-right\"><img src=\"\/eng\/files\/2023\/05\/Zeiss-XRADIA-with-people-477x636-1.jpg\" alt=\"Zeiss XRADIA\" \/><div class=\"bu-slide-caption caption-bottom-right\"><p class=\"bu-slide-caption-title\">Zeiss Xradia 410 Versa System<\/p><\/div><\/div><\/li><li id=\"bu-slideshow-139697_3\" class=\"slide \"><div class=\"bu-slide-container slide-caption-bottom-right\"><img src=\"\/eng\/files\/2023\/05\/Asylum-afm_2-1-e1486403807313-358x636-1.jpg\" alt=\"AFM-FM Microscope\" \/><div class=\"bu-slide-caption caption-bottom-right\"><p class=\"bu-slide-caption-title\">AFM-FM Microscope<\/p><\/div><\/div><\/li><li id=\"bu-slideshow-139697_4\" class=\"slide \"><div class=\"bu-slide-container slide-caption-bottom-right\"><img src=\"\/eng\/files\/2023\/05\/Renishaw-Raman-Microscope_1-636x358-1.jpg\" alt=\"Rensihaw Raman Microscope\" \/><div class=\"bu-slide-caption caption-bottom-right\"><p class=\"bu-slide-caption-title\">Renishaw Raman Microscope System<\/p><\/div><\/div><\/li><li id=\"bu-slideshow-139697_5\" class=\"slide \"><div class=\"bu-slide-container slide-caption-bottom-right\"><img src=\"\/eng\/files\/2023\/05\/FIB_operated-768x432-1.jpg\" alt=\"FEI Quanta 3D\" \/><div class=\"bu-slide-caption caption-bottom-right\"><p class=\"bu-slide-caption-title\">Jeremy Reeves (Postdoctoral Associate in Professor Bishop\u2019s group) is patterning MEMS structures using FEI FIB system.<\/p><\/div><\/div><\/li><li id=\"bu-slideshow-139697_6\" class=\"slide \"><div class=\"bu-slide-container slide-caption-bottom-right\"><img src=\"\/eng\/files\/2023\/05\/FEI_TEM-358x636-1.jpg\" alt=\"FEI Osiris\" \/><div class=\"bu-slide-caption caption-bottom-right\"><p class=\"bu-slide-caption-title\">FEI Osiris TEM\/STEM microscope<\/p><p class=\"bu-slide-caption-text\">for microstructural investigations on nanoscale<\/p><\/div><\/div><\/li><li id=\"bu-slideshow-139697_7\" class=\"slide \"><div class=\"bu-slide-container slide-caption-bottom-right\"><img src=\"\/eng\/files\/2024\/09\/PLD-Photo-Overview-636x477.jpg\" alt=\"\" \/><div class=\"bu-slide-caption caption-bottom-right\"><p class=\"bu-slide-caption-title\">PLD System<\/p><\/div><\/div><\/li><li id=\"bu-slideshow-139697_8\" class=\"slide \"><div class=\"bu-slide-container slide-caption-bottom-right\"><img src=\"\/eng\/files\/2024\/09\/PLD-Photo-Target-Laser-Ablation-in-Vaccum-Chamber-477x636.jpg\" alt=\"\" \/><div class=\"bu-slide-caption caption-bottom-right\"><p class=\"bu-slide-caption-title\">PLD System<\/p><\/div><\/div><\/li><\/ul><\/div><div class=\"bu-slideshow-navigation-container\"><ul class=\"bu-slideshow-navigation nav-icon\" id=\"bu-slideshow-nav-139697\" aria-hidden=\"true\"><li><a href=\"#\" id=\"pager-1\" class=\" active\" aria-hidden=\"true\"><span>1<\/span><\/a><\/li> <li><a href=\"#\" id=\"pager-2\" class=\"\" aria-hidden=\"true\"><span>2<\/span><\/a><\/li> <li><a href=\"#\" id=\"pager-3\" class=\"\" aria-hidden=\"true\"><span>3<\/span><\/a><\/li> <li><a href=\"#\" id=\"pager-4\" class=\"\" aria-hidden=\"true\"><span>4<\/span><\/a><\/li> <li><a href=\"#\" id=\"pager-5\" class=\"\" aria-hidden=\"true\"><span>5<\/span><\/a><\/li> <li><a href=\"#\" id=\"pager-6\" class=\"\" aria-hidden=\"true\"><span>6<\/span><\/a><\/li> <li><a href=\"#\" id=\"pager-7\" class=\"\" aria-hidden=\"true\"><span>7<\/span><\/a><\/li> <li><a href=\"#\" id=\"pager-8\" class=\"\" aria-hidden=\"true\"><span>8<\/span><\/a><\/li> <li><a href=\"#\" id=\"pager-9\" class=\"\" aria-hidden=\"true\"><span>9<\/span><\/a><\/li> <\/ul><\/div><\/div>\n<div class=\"bu_collapsible_container \" aria-live=\"polite\" data-customize-animation=\"false\"><h3 class=\"bu_collapsible\" aria-expanded=\"false\"tabindex=\"0\" role=\"button\">Pulsed Laser Deposition (PLD) System<\/h3><div class=\"bu_collapsible_section\" style=\"display: none;\"><\/p>\n<p>This advanced equipment allows us to grow high-quality oxide thin films right here on campus, opening up a world of research opportunities for our faculty and students. Initiated by Professor Soumendra Basu and PhD candidate Emily Ghosh, and maintained by Paul Mak of the Photonics Center and MSE, anyone will have the chance to buy their own supplies and grow their own thin films.<\/p>\n<p>Professor Basu shared, &#8220;There are numerous applications for this equipment, and many faculty members and researchers are working on different projects that will benefit greatly from having this resource on hand.\u201d<\/p>\n<p>Graduate students will be trained as &#8220;superusers&#8221; to help new users get started, under the guidance of our photonics staff. Special shoutout to Emily Ghosh and Professor Basu for their hard work in bringing this cutting-edge technology to our division!<\/p>\n<p>Stay tuned for more updates on this exciting addition. For inquiries, reach out to Professor Basu at basu@bu.edu.<\/p>\n<p><strong>More info about the PLD system: <\/strong><\/p>\n<p>Pulsed Laser Deposition (PLD) is a physical vapor deposition process used to fabricate high quality thin films in ultra-high vacuum. A high-power pulsed laser is used to ablate a target material, forming a vapor plume of the target&#8217;s material. The plume interacts with the tailored gas environment of the chamber to create a plasma of the material that then deposits on the substrate to form a thin film.<\/p>\n<p>This technique allows for thin film deposition of a wide range of complex materials, such as complex oxides used in the solid oxide cell electrodes, that could otherwise not be easily fabricated using other physical vapor deposition techniques.<\/p>\n<p>In-situ characterization techniques, such as reflection high-energy diffraction (RHEED), can be used in conjunction with the deposition to provide real-time information about the growth mechanisms of the films.<\/p>\n<p><\/div>\n<\/div>\n\n<div class=\"bu_collapsible_container \" aria-live=\"polite\" data-customize-animation=\"false\"><h3 class=\"bu_collapsible\" aria-expanded=\"false\"tabindex=\"0\" role=\"button\">Bruker X-Ray Systems<\/h3><div class=\"bu_collapsible_section\" style=\"display: none;\"><br \/>\nTwo <strong>Bruker X-Ray systems<\/strong> have been acquired by an NSF MRI award led by Prof. Ludwig, and are available for faculty use. Dr. Jeffrey Bacon (Chemistry) <a href=\"mailto:jwbacon@bu.edu\">(jwbacon@bu.edu<\/a>) oversees training and maintenance on these two systems. The N8 Horizon and the D8 Discover systems are complementary, and allow for small- and wide-angle X-ray scattering (SAXS and WAXS).<br \/>\nThe <strong>N8 Horizon<\/strong>, introduced by Bruker in 2012, is one of the first such systems installed in the US. The instrument is designed for compact spaces and has transmission and grazing incidence SAXS capabilities.<br \/>\n<\/div>\n<\/div>\n\n<div class=\"bu_collapsible_container \" aria-live=\"polite\" data-customize-animation=\"false\"><h3 class=\"bu_collapsible\" aria-expanded=\"false\"tabindex=\"0\" role=\"button\">D8 Discover WAXS System<\/h3><div class=\"bu_collapsible_section\" style=\"display: none;\"><\/p>\n<p>The <strong>D8 Discover<\/strong> is a very versatile WAXS system with general x-ray diffraction (XRD), high-resolution XRD, reciprocal space mapping, grazing incidence diffraction, x-ray reflectivity, pole-figure analysis, and sample heating (1000\u00b0C) capabilities.<br \/>\n<\/div>\n<\/div>\n\n<div class=\"bu_collapsible_container \" aria-live=\"polite\" data-customize-animation=\"false\"><h3 class=\"bu_collapsible\" aria-expanded=\"false\"tabindex=\"0\" role=\"button\">Zeiss Xradia 410 Versa System<\/h3><div class=\"bu_collapsible_section\" style=\"display: none;\"><\/p>\n<p>A <strong>Zeiss Xradia 410 Versa system<\/strong> was acquired and set up through a separate NSF MRI award, led by Professor Elise Morgan (ME, BME, MSE) (<a href=\"mailto:efmorgan@bu.edu\">efmorgan@bu.edu<\/a>).\u00a0 This tool bridges the gap between high-performing X-ray microscopy (XRM) and less powerful computed tomography (CT) systems. This system provides quantitative 3-D characterization of materials microstructure at multiple length scales down to the sub-micron, including porosity, density, surface area, and topological measures such as 3-D connectivity.<br \/>\n<\/div>\n<\/div>\n\n<div class=\"bu_collapsible_container \" aria-live=\"polite\" data-customize-animation=\"false\"><h3 class=\"bu_collapsible\" aria-expanded=\"false\"tabindex=\"0\" role=\"button\">AFM-FM Microscope<\/h3><div class=\"bu_collapsible_section\" style=\"display: none;\"><\/p>\n<p>The <strong>AFM-FM Microscope<\/strong> that was housed in the core facility is currently undergoing major improvements via a third NSF MRI award led by Professor Bennett Goldberg (Physics, BME, ECE, MSE). In conjunction with Asylum, the system is being retrofitted with Raman Spectroscopy for enhanced tip capability.<br \/>\n<\/div>\n<\/div>\n\n<div class=\"bu_collapsible_container \" aria-live=\"polite\" data-customize-animation=\"false\"><h3 class=\"bu_collapsible\" aria-expanded=\"false\"tabindex=\"0\" role=\"button\">Renishaw Raman Microscope<\/h3><div class=\"bu_collapsible_section\" style=\"display: none;\"><\/p>\n<p>Next to the AFM is a new <strong>Renishaw Raman Microscope system<\/strong> that includes a heating\/cooling stage and multiple wavelengths for Raman observation. This tool was purchased via the Photonics Center Capital Equipment Committee and is open to all Photonics and Materials Science &amp; Engineering faculty.<br \/>\n<\/div>\n<\/div>\n\n<div class=\"bu_collapsible_container \" aria-live=\"polite\" data-customize-animation=\"false\"><h3 class=\"bu_collapsible\" aria-expanded=\"false\"tabindex=\"0\" role=\"button\">Focused Ion Beam\/Transmission Electron Microscope Facility<\/h3><div class=\"bu_collapsible_section\" style=\"display: none;\"><br \/>\nIn the basement of the Photonics Center, the <strong>Focused Ion Beam\/Transmission Electron Microscope Facility<\/strong> is comprised of two laboratories consisting of 600 square feet, and is overseen by Dr. Alexey Nikiforov (Photonics) (<a href=\"mailto:alnik@bu.edu\">alnik@bu.edu<\/a>). This laboratory houses a recently purchased FEI Quanta 3D FEG FIB (Field Emission Gun Focused Ion Beam) system and a FEI Tecnai Osiris 200kV S\/TEM (Scanning\/Transmission Electron Microscope).<\/p>\n<p>The <strong>FEI Quanta 3D FEG FIB<\/strong> is a powerful tool for SEM (Scanning Electron Microscope) imaging to aid removal and deposition of materials at a micro\/nano scale with a resolution of 1.2 nm in the HiVac mode, 2.9 nm in LoVac mode, and 7 nm with the FIB column. The system includes gas injector modules (GIS) and an Omniprobe micromanipulator can be used for TEM sample preparation and lift-out. A Peltier\/Heating Stage Control Kit allows for the study of <em>in situ <\/em>dynamic behavior of materials at different humidity (up to 100% RH) and temperatures (-10\u00b0C to 1000\u00b0C).<br \/>\n<\/div>\n<\/div>\n\n<div class=\"bu_collapsible_container \" aria-live=\"polite\" data-customize-animation=\"false\"><h3 class=\"bu_collapsible\" aria-expanded=\"false\"tabindex=\"0\" role=\"button\">FEI Tecnai Osiris 200V S\/TEM<\/h3><div class=\"bu_collapsible_section\" style=\"display: none;\"><\/p>\n<p>The <strong>FEI Tecnai Osiris 200V S\/TEM<\/strong> is a versatile scanning transmission electron microscope that allows for bright-field\/dark-field imaging, selected area and convergent beam diffraction, and high-resolution imaging with a point-to-point resolution of 0.25nm, and line resolution of 0.102 nm, extended to 0.16 nm with TrueImage\u2122 software, and a STEM resolution of 0.18 nm. The system can seamlessly switch between TEM and STEM modes. The system also includes energy dispersive x-ray (Super-X EDX) capabilities for composition analysis and mapping, and energy filtered TEM with electron energy loss spectroscopy (Gatan EELS) for light element quantification and mapping.<\/p>\n<p><\/div>\n<\/div>\n\n<div class=\"bu_collapsible_container \" aria-live=\"polite\" data-customize-animation=\"false\"><h3 class=\"bu_collapsible\" aria-expanded=\"false\"tabindex=\"0\" role=\"button\">Sample Prep Room<\/h3><div class=\"bu_collapsible_section\" style=\"display: none;\"><br \/>\n<strong>A new sample preparation room<\/strong> to prepare electron transparent samples for use in the TEM is currently operational and open to all Photonics and Materials Science &amp; Engineering faculty. Through equipment purchases at the Photonics Center, a <strong>grinder, cut-off saw, disc cutter, automated polishing and lapping equipment, dimpler, and ion mill<\/strong> are all installed.<\/p>\n<p><strong>The materials processing area is comprised of two Salare hoods<\/strong> that are dedicated to acid and base processing. Table space is provided within this room to allow for sample preparation and oven use if applicable.<br \/>\n<\/div>\n<\/div>\n\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>The Materials Science &amp; Engineering Core Research Facility was officially commissioned in June 2012. Since that time, it has grown to house multiple core pieces of equipment for the Materials Science &amp; Engineering and Photonics Center community. Address: 8 Saint Mary\u2019s St., Rooms 603 &amp; 605, Boston, MA 02215 Lab Oversight: Professor David Bishop, djb1@bu.edu, [&hellip;]<\/p>\n","protected":false},"author":9305,"featured_media":0,"parent":118511,"menu_order":6,"comment_status":"closed","ping_status":"closed","template":"page-templates\/no-sidebars.php","meta":[],"_links":{"self":[{"href":"https:\/\/www.bu.edu\/eng\/wp-json\/wp\/v2\/pages\/118529"}],"collection":[{"href":"https:\/\/www.bu.edu\/eng\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/www.bu.edu\/eng\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/www.bu.edu\/eng\/wp-json\/wp\/v2\/users\/9305"}],"replies":[{"embeddable":true,"href":"https:\/\/www.bu.edu\/eng\/wp-json\/wp\/v2\/comments?post=118529"}],"version-history":[{"count":11,"href":"https:\/\/www.bu.edu\/eng\/wp-json\/wp\/v2\/pages\/118529\/revisions"}],"predecessor-version":[{"id":155956,"href":"https:\/\/www.bu.edu\/eng\/wp-json\/wp\/v2\/pages\/118529\/revisions\/155956"}],"up":[{"embeddable":true,"href":"https:\/\/www.bu.edu\/eng\/wp-json\/wp\/v2\/pages\/118511"}],"wp:attachment":[{"href":"https:\/\/www.bu.edu\/eng\/wp-json\/wp\/v2\/media?parent=118529"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}